EXTECH pH Conductivity TDS Salinity Temperature Meter User Manual

EXTECH pH Conductivity TDS Salinity Temperature Meter

Introduction

Congratulations on your purchase of the ExStik® EC500 pH/Conductivity/Total Dissolved Solids (TDS) / Salinity meter. With the EC500’s dynamic cell-constant technology it is possible to measure a wide range of Conductivity, TDS, and Salinity with the same electrode. Careful use and maintenance will provide years of reliable service.

Powering the ExStik™

The ExStik® uses four (4) CR2032 Lithium Ion Batteries (included). If the batteries are weak, the ‘BAT’ indicator appears on the LCD. Press the ON/OFF key to turn the ExStik® on or off. The auto power off feature shuts the ExStik® off automatically after 10 minutes of inactivity to preserve battery life.

Getting Started

Remove the cap from the bottom of the ExStik to expose the pH electrode, reference junction and conductivity electrodes.
Before the first use or after storage, soak the electrode in tap water or pH 4 buffer solution for about 10 minutes.
White KCL crystals may be present in the cap or on the electrode. This is to be expected depending on the length of time in storage. These crystals will dissolve while soaking the electrode or they can be rinsed away with tap water.
For best results calibrate with pH 7 buffer solution first, then calibrate with the buffer solution closest to the expected pH value of the solution or material to be tested.
To preserve the pH electrode life, keep the sponge in the protective cap soaked with tap water or pH 4 buffer solution.
For best results, calibrate for conductivity with a standard in the expected range of the sample.For maximum accuracy calibrate from low conductivity value standards to high value standards.

Meter Description

Front Panel Description

Battery compartment cover
LCD Display
MODE/HOLD button
CAL/RECALL button
ON/OFF button
Electrode Collar
pH/Conductivity Electrode

(Note: The Electrode cap is not shown)

LCD Display

Bargraph display
Measurement units
Main display
Range calibration and low battery indicators
Temperature display
Renew indicator
Reading hold indicator

Measurement Procedure

Sample Preparation

For Conductivity, TDS or Salinity place the test sample in a sample cup with enough depth (2.5cm minimum) to cover the electrode. Stir the solution to remove any air bubbles.
For pH, place the tip of the electrode in the sample or make contact with a wet surface.

Measurement

Press the ON button. ( and then “SELF CAL” will appear in the display during the turn-on diagnostics)
Depress and hold the MODE/HOLD key to scroll to the desired measurement mode.
Insert the electrode into the sample making sure that the electrodes are completely submersed.
Slowly stir the solution with the electrode to remove air bubbles if in the Conductivity, TDS or Salinity mode.
If in the Conductivity, TDS or Salinity modes, the meter will auto-range to the proper range and then display the reading.

Changing Measurement Function

The meter can be set to measure pH, Conductivity, TDS or Salinity.To change the mode:

Press and Hold the MODE/HOLD button for 2 seconds and the display will begin to scroll through the units.µS (Conductivity); pH; ppm S (Salinity); ppm (TDS); mg/l (TDS);Note: The “HOLD” function cannot be on when changing the measurement function. If “HOLD” is displayed in the lower left corner of the display, briefly press the MODE/HOLD button to turn it off.
When the desired units are displayed, release the MODE/HOLD button.

TDS Compensation Ratio

The TDS value is determined by multiplying a conductivity reading by a known ratio factor. The meter allows for selecting a conversion ratio in the range of 0.4 to 1.0. The ratio varies with the application, but is typically set between 0.5 and 0.7.Note: The stored ratio will briefly appear in the lower temperature display when the meter is first turned on, or when changing measurement function to TDS.

Note: In the Salinity mode the ratio is 0.4 to 0.6 auto

To change the ratio, while in the TDS measurement mode (ppm or mg/l):

Press and release the CAL/RECALL button twice in succession. The stored ratio will appear in the display.
Press the MODE/HOLD button to increase the ratio value in steps of 0.1.
When the desired ratio is displayed, press and release the CAL/RECALL button to store the value and return to the normal mode.
If no buttons are pressed for 5 seconds, the meter returns to measure mode.

Storing Readings

Press the MODE/HOLD button to store a reading. The storage location number will be displayed on the lower display, while the main display shows the stored reading. The meter will enter the HOLD mode and the “HOLD” indicator will appear.
Press the MODE/HOLD button again to exit the HOLD mode and return to normal operation.
If more than 25 readings are stored, previously stored readings (starting with number 1) will be overwritten.

Recalling Stored Readings

Press the CAL/RECALL button and then press the MODE/HOLD button. A location number (1 through 25) will briefly appear and then the value stored in that location will appear. The displayed units will flash, indicating that the storage recall mode is active.
The last stored reading will be displayed first. Pressing and releasing the MODE/HOLD button will scroll through the stored readings one at a time. The location number is displayed first followed by the reading stored in that location.
To exit the storage mode, press the CAL/RECALL button and the meter will return to normal operation, after displaying “End”.

Clear Stored Memory

With the unit on, press and hold ON/OFF for 4 seconds. “clr” will be briefly displayed when the memory is cleared.

Changing Temperature Units

To change the displayed temperature units (°C or °F):

With the unit OFF, press and hold down the CAL/RECALL button.
With the CAL/RECALL button depressed momentarily press the ON/OFF button. When “SELF CAL” appears in the display release the CAL/RECALL button. The unit will power on with temperature displayed in the new units.

Data Hold Mode

Press the MODE/HOLD button to hold (freeze) a reading in the display. The meter will enter the HOLD mode and the “HOLD” indicator will appear.Note: This also stores the reading.Press the MODE/HOLD button again to return to normal operation.

Auto Power OFF

The auto power off feature automatically shuts the meter off 10 minutes after the most recent button press.

Auto Power OFF Disable

To disable the Auto Power Off feature:

Turn the unit on
Press CAL/RECALL once (Quickly)
Immediately and simultaneously press the MODE/HOLD and ON/OFF buttons for approximately 2 seconds, until “OFF” is briefly displayed

To disengage this feature, turn the unit off with the ON/OFF button. The next time the unit is powered up, Auto Power OFF mode will be engaged again.

Low Battery Indication

When the batteries become weak the “BAT” icon will appear in the display. Refer to the Maintenance section for battery replacement information.

Calibration – pH (1, 2, or 3 points)

Place the electrode into a buffer solution (4, 7, or 10). Press and hold the CAL/RECALL key until “CAL” appears in the lower (temp.) display. When doing a 2 or 3 point calibration, calibrate with pH 7 buffer first, then follow with pH 4 then the pH 10 buffer.
The ExStik® automatically recognizes the solution and calibrates itself to that value (the circled number on the LCD will match the solution). Note that if the solution is more than 1 pH unit off from the L (4), M (7), or H (10) pH buffer, or if the electrode slope is low, the ExStik ® will assume an error and abort the calibration (‘End’ will be displayed, and the unit will return to measure mode.)
During calibration, the pH reading flashes on the main display.
When calibration is complete, the ExStik® automatically displays “SA”, then “End” and returns to normal operation mode.
The appropriate circled indicator (L, M, or H) appears on the LCD when a particular calibration or series of calibrations has been completed within one power on cycle. When the ExStik® is turned off, the circled indicator configuration and the calibration data will be retained.
For a two or three-point calibration, repeat steps 1-4.
See Reset Calibration Data to clear all calibration data from the meter.

CAL Reminder Display

When in pH measurement mode, a “CAL” icon will appear after 15 on/off cycles of the meter without performing a calibration. The CAL display is simply a reminder to calibrate pH, and will turn off when the pH electrode is recalibrated. The reminder does not affect function in any way.

RENEW Display

A flashing ‘RENEW’ warning indicates that the probe is not performing to expected specifications. If cleaning and recalibration does not cause the RENEW icon to disappear, replace the probe (see optional accessories on the last page of this manual). The RENEW display appears as a result of the pH electrode slope falling below 70% of a nominal slope.

Measurement and Display Considerations

If the unit appears to be locked (display frozen). It is possible that the Data Hold mode has been inadvertently accessed by pressing the MODE/HOLD button. (“HOLD” will be displayed in the bottom left of the LCD.) Simply press the MODE/HOLD button again or turn the meter off and then on.
For maximum accuracy, allow sufficient time for the temperature of the probe to reach the temperature of the sample before calibrating. This will be indicated by a stable temperature reading on the display.

Reset Calibration Data

Follow this procedure to clear all calibration data from the meter. Resetting the calibration data may be necessary when new calibration solutions are used or accuracy of measurements is in question.

Turn off the meter.
Press and Hold the Cal/Recall and Mode/Hold buttons.
Momentarily press the On/Off button, as soon as the display comes on, release all 3 buttons.
The display will show “dFLt rSt” (default reset) and all of the calibration data will be erased. If “dFLt rSt” does not appear, retry the procedure.
Proceed to the calibration routine for pH and Conductivity.

Calibration – Conductivity

Meter accuracy verification should be performed on a periodic basis. Once per month is the recommended cycle for normal use. If calibration is required, a conductivity standardizing solution must be obtained. The meter can be calibrated in any or all of the three ranges. Standardizing solutions of 84µS/cm, 1413µS/cm or 12.88mS/cm (12,880µS/cm) are used for the automatic calibration recognition procedure. No other calibration values are permitted.Calibration is always done in conductivity mode. Since salinity and TDS values are calculated from conductivity values, this procedure also calibrates the salinity and TDS ranges.

Fill a sample cup with the standardizing solution.
Turn the meter ON and insert the electrode into the solution. Tap or move the electrode in the sample to dislodge any air bubbles.
Press and hold the CAL/RECALL button (approximately 2 seconds) until “CAL” appears in the lower (temp) display. The main display will start flashing.
The meter will automatically recognize and calibrate to the standardizing solution. The display will briefly indicate “SA”, End and then return to the measurement mode after a calibration.Note: The “SA” will not appear if the calibration fails.
The “range calibrated” symbol will appear in the display for each range that is calibrated during that power on cycle. Low range, 84µS/cm Medium range, 1413µS/cm High range, 12.88mS/cm (12,880µS/cm)

Note: Each time the calibration mode is entered all calibration symbols on the display are cleared, but only the calibration data for the currently calibrated range is replaced. The other two ranges keep the existing calibration data, just the symbols are removed. Calibration of all three ranges must be performed during one power on period for all three range calibration symbols to appear.

See Reset Calibration Data to clear all calibration data from the meter.Note: The meter allows for a 1, 2 or 3 point calibration. If calibration is done for more than one point the lowest value standard should be done first to obtain the best accuracy

Considerations and Techniques

Do not touch the inner surfaces of the conductivity electrodes. Touching the surface of the platinized electrodes may damage and reduce the life of the probe.
Store the electrode in the wetting cap with the sponge moistened with pH 4.01 buffer solution.
Always rinse the electrode in de-ionized water between measurements to avoid cross contamination of the sample. Double rinsing is recommended when high accuracy is required.
Periodically, accumulated salt deposits from the reference electrode may build up in the storage cap, and should be rinsed away. These deposits could affect measured values of low conductivity samples.
When measuring low conductivity samples, extra care is recommended in rinsing the probe to avoid contamination of the sample with electrolyte from the pH reference electrode. This will only be a factor when measuring in the low range, and can be further minimized by increasing the volume of the sample. (Example: Try a 200 to 500 mL sample.)
If the 20mL sample cup is to be used, then the electrode should not be allowed to sit in the sample for any longer than necessary, to avoid pH electrolyte leakage into the sample, raising the conductivity value.

Operational Matrix

*Function / Resulting Action*	*Power Status*	*Mode Setting*	*Required Key Press Sequence*
On/Off	On or Off	Any	Momentary press of the ON/OFF key
Calibration	On	pH or Conductivity	Press & hold CAL/RECALL key for 2 seconds, until it enters CAL function
Store Reading	On	Any measure mode	Momentary press of the MODE/HOLD key
Hold Release	On	While In Hold Mode	Momentary press of the MODE/HOLD key
Enter Memory Retrieval	On	Any measure mode	Momentary press of the CAL/RECALL key followed by a momentary press of the MODE/HOLD key (Within 4 seconds)
Scroll Stored Readings	On	Memory Recall	Momentary press of the MODE/HOLD key (Displays “last in first out”)
Exit Memory Retrieval	On	Memory Recall	Momentary press of the CAL/RECALL key
Clear Stored Memory	On	Any Measure Mode	Press and hold the ON/OFF key for 4 seconds, until “clr” is displayed.
Change Measurement Mode	On	Any	Press and hold the MODE/HOLD key for at least 2 seconds (the modes will scroll by until the key is released)
Enter Cond/TDS Ratio	On	TDS (ppm or mg/l)	Press and release the CAL/RECALL key twice in quick succession
Change Cond/TDS Ratio	On	TDS ratio	Momentary press of the MODE/HOLD key (each key press increases the ratio by 0.1, the value cycles from 0.4 – 1.0)
Exit Cond/TDS Ratio	On	TDS ratio	Momentary press of the CAL/RECALL key
Change Temperature Units	Off	n/a (off mode)	Press and hold the CAL/RECALL key then momentarily press the On/Off key. Release the CAL/RECALL key after the “SELF CAL” lights
Override Auto Power Off	On	Any measure mode	Momentarily press the CAL/RECALL key then simultaneously press and hold the ON/OFF & MODE/HOLD key for approximately 2 seconds, until “oFF” is displayed
Default Reset	OFF	n/a	Simultaneously press ON/OFF, CAL/RECALL and MODE/HOLD momentarily. “dFLt” will be displayed.

Specifications

Display	2000 count LCD with Bargraph
pH Range	0.00 to 14.00
pH Accuracy	±0.01 pH typical
pH ATC Range	32°F to 194°F (0°C to 90°C)
pH Reference Junction	Permanent gel, non-refillable
Conductivity ranges	0 to 199.9µS200 to 1999µS2.00 to 19.99mS
TDS ranges (Variable ratio)	0 to 99.9ppm or mg/L1.00 to 9.99ppt or g/L
Salinity range	0 to 99.9ppm100 to 999ppm1.00 to 9.99ppt
TDS Ratio	0.4 to 1.0 adjustable
Salinity Ratio	0.4 to 0.6 auto
Conductivity ATC	2.0% per °C
Conductivity ATC Range	32.0°F to 140oF (0.0°C to 60.0°C)
Temperature Range	23.0°F to 194°F (-5.0°C to 90.0°C)
Temperature Resolution	0.1 up to 99.9, 1 >100
Temperature Accuracy	±1.8°F; 1°C (from 23 to 122°F; -5 to 50°C)±5.4°F; 3°C (from122 to 194°F; 50 to 90°C)
Accuracy	Conductivity: ±2% full scaleTDS: ±2% full scaleSalinity: ±2% full scale
Measurement Memory	25 tagged (numbered) readings
Low battery indication	‘BAT’ appears on the LCD
Power	Four (4) CR2032 Lithium-Ion Batteries
Auto power off	After 10 minutes (override available)
Operating conditions	23°F to 122oF (-5°C to 50oC)
Dimensions	1.6 x 7.9 x 1.6” (40 x 200 x 40 mm)
Weight	3.3 oz (93 g)

Maintenance

Battery Replacement

Twist off the battery compartment cap
Holding the battery housing in place with a finger, pull out the battery carrier using the two small tabs.
Replace the four (4) CR2032 batteries observing polarity.
Replace the battery compartment capSafety: Please dispose of batteries responsibly; never dispose of batteries in a fire, batteries may explode or leak. If the meter is not to be used for 60 days or more, remove the battery and store separately

Electrode Replacement

To remove an electrode, unscrew and completely remove the electrode collar (turn the collar counter-clockwise to remove).
Gently rock the electrode from side to side, pulling it downwards, until it disconnects from the meter.
To attach an electrode, carefully plug the electrode into the meter socket (note that the electrode connector is keyed, ensuring proper connection).
Tighten the electrode collar firmly enough to make a good seal (a rubber gasket seals the electrode with the meter).

Cleaning Recommendations

When cleaning the probe, take care not to scratch or damage the sensing surface or the platinized electrode surfaces.

*Contaminant*	*Cleaning Solution*	*Instructions*
Water soluble substances	Deionized water	Soak or scrub with a soft brush. Recondition in 4 or 7 buffer for 1 hour.
Grease & Oil	Warm water and household detergent	Soak or scrub with a soft brush, maximum of 10 minutes. Rinse thoroughly with DI water, recondition in 4 or 7 buffer for 1 hour.
Heavy grease & Oil	Alcohol	Maximum of 5 minute soak, scrub with a soft brush. Rinse thoroughly with DI water, recondition in 4 or 7 buffer for 1 hour.
Lime and hydroxide coatings	10% acetic acid	Soak until coating dissolved, maximum of 5 minutes. Rinse thoroughly with DI water, recondition in 4 or 7 buffer for 1 hour.

Please Note: Since the EC500 does not have a refillable pH reference electrolyte chamber, it is important not to soak the electrode in the above solutions for more than the recommended times. To do so may cause a reference potential shift, which will cause degradation in performance or failure.

Troubleshooting

*Problem*	*Possible Cause*	*Action*
Reading is frozen	Unit is in “HOLD” mode	Press MODE/HOLD key to exit “HOLD” mode
“BAT” message	Batteries are low	Replace batteries
Unit will not calibrate in pH	Low pH slope	Replace electrode, see reorder information
Unit will not calibrate in pH	Clogged or contaminated reference junction	Clean junction (see cleaning instructions)
Unit will not calibrate in pH	Damaged or worn out sensing membrane	Replace electrode, see reorder information
Unit will not calibrate in pH	Contaminated pH buffers	Use fresh buffers
Unit will not calibrate in conductivity mode	Contaminated conductivity standards	Use fresh standards
Unit will not calibrate in conductivity mode	Dirty probe	Clean conductivity probe (See cleaning instructions)
Unit will not calibrate in conductivity mode	Damaged conductivity probe	Replace electrode, see reorder information
Unit will not calibrate in conductivity mode	Trapped air bubbles	Tap or stir to release air bubbles
Unit will not turn on	Batteries are low or dead	Replace batteries
Unit will not turn on	Batteries installed with incorrect polarity	Replace batteries, observe polarity
“RENEW” message	pH sensor needs recalibration	Recalibrate unit Use fresh buffers
“RENEW” message	pH sensor slope has fallen below acceptable limits	Replace electrode, see reorder information
Unit will not respond to any key presses	Internal fault	Perform hard reboot: Remove batteries, hold ON/OFF switch down for 5 seconds, replace batteries

Two-year Warranty

FLIR Systems, Inc. warrants this Extech brand instrument to be free of defects in parts and workmanship for two years from date of shipment (a six-month limited warranty applies to sensors and cables). To view the full warranty text please visit: http://www.extech.com/support/warranties.

Calibration and Repair Services

FLIR Systems, Inc. offers calibration and repair services for the Extech brand products we sell. We offer NIST traceable calibration for most of our products. Contact us for information on calibration and repair availability, refer to the contact information below. Annual calibrations should be performed to verify meter performance and accuracy. Product specifications are subject to change without notice. Please visit our website for the most up-to-date product information: www.extech.com.

Contact Customer Support

Customer Support Telephone List: https://support.flir.com/contactCalibration, Repair, and Returns: [email protected]Technical Support: https://support.flir.com

References

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Posted

2023-01-18

EXTECH

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Tags:

ExStik EC500, EXTECH, pH Conductivity TDS Salinity Temperature Meter